Removing BA from "solution"

[Ulter]

I depends on the test. If you're cooking Enanthate, which can literally melt in your hand, you should stay at 175deg for 10 minutes, three times. But it's rare that you'd need to do that for Enanthate.
For everything else 250deg for 10 minutes, three times is fine. You don't need to boil or melt anything. Alcohol evaporates pretty easily so heating it up a little in the oven just accelerates this process.
Some people do it one time for 20 min but my pins always melt shut when I do that.

 

[PolfaJelfa]

Yup Ulter u read my mind, its Enthanate..which seems to suck in this case.

 

[shamrock11]

Ok! Polfa I apologize for the information I gave you. I was going just off the basic proterties on alcohols without looking up the structure. They are right it does have a boiling point of 205 degrees C. I have never heard of a boiling point this high unless the alcohol is attached to a ring and in this case it is. So there is no way you can boil it off. I can figuer some ways to seperate it from the test, but then it wouldn't be sterile anymore. I just wanted to apologize for the info before I looked at the structure. If you have anymore chemical type questions feel free to ask me or PM me. It's usually not like me to give info. without looking into it first so again I apologize.

 

[PolfaJelfa]

Ok , broly no prob.
What other way do you think i can use? And believe me i think this **** will remain sterile...its got Way too much BA inside....2x as much as its supposed to be.

 

[PolfaJelfa]

205 degrees..i think the glass might break at that temp...and the 18g plastic will melt.....there has got to be a way to do this.

 

[Ulter]

The vial won't break at 200deg or even 300deg and if you keep it short the plastic on the pin won't close. Keep in mind, like I said, you're not trying to boil it. You're just going to accelerate the evaporation of the alcohol by doing this.

 

[shamrock11]

Well the problem is heat is not going to help at all. We are talking about 205 degrees celsius, which converts to about 400 degrees fahrenheit.Trying to evaporate at this temp is going to be diffcult. There is no boiling point listed for the tests, but I would say that looking at it's structure it will be very high if at all. What exactly did you do to get too much BA and what was the actual solution suppose to be. I need this information to help you more.

 

[Ulter]

Well the problem is heat is not going to help at all.

The problem is that you've never done this so you don't what you're talking about. We've been cooking off excess solvent in gear for several years. It's not a new experiment. Many times the solvent will evaporate right in the vial without ANY heat or ventilation. This is witnessed by those who have AS that sits for a long time and suddenly they see the material fall right out of the solvent and appear as crystals or powder at the bottom of the vial.

The temperatures I wrote are F not C. It doesn't take much heat to accelerate the evaporation process.

There is no boiling point listed for the tests,

Of course there is a list of test ester melting points. Several as a matter of fact.
HE didn't do anything to get too much solvent in the vial. The underground manufacturers don't work in a Clean Room so they make it up by adding more solvent. They also put more material in it than there should be to get high concentrations that people want. The only way to do that is to use a ridiculous amount of solvent.

 

[PolfaJelfa]

1st of all im going to have to go by Ulters advice....i believe you realy know what you are talking about like always. Second...actually Ulter..it was my fault...i put the excess Ba in there.....and btw i never use any underground manufacturers.... only Human Grade....and myself construed. The excess Ba is due to someone puting the Ba in there be4 , i basically did it again.

 

[Ulter]

I don't know what to say. I stand corrected. I have never heard of anyone adding BA to their vial. What on God's earth posessed you to do that?