need help asap

[thelocal]

well this is what happened also,i read the melting pint on decca is low,so i use a hairdryer when i first got it to test the powder to see if it was legit,it was,then i froze is to make it solid for a few mins..put it up at room temp,when i was ready to make it the powder was hard and clumpy,i tried melting it first with the hairdryer wasnt going so wel so i just put it in the beaker with the ba and bb on a skillet wiht a little water on the stove,my bro did turn it to high and it bubble once(was at boiling point for a brief second) but i didnt see any water splash or anything

 

[HAYEZ]

sounds to me like you got some moisture in the powder and thats what the cloudiness is coming from... i would take one of the vials stick a needle tip in it to vent and throw it in the oven at 250 for 30 minutes...see if that works..if it looks to improve after that but there is still some in it then do it again..

once you sort it out then do it to all of them...next time dont fuck with ur gear!!!!! hahahahahahahah but that should take care of it...let me know what happens and dont freeze it to cool it...let it cool on its own..then see whats up

 

[thelocal]

lol yea i know huh.man i have done that seval times last night it didnt improve,...i am thinking of drawing it all out,putting it back in the beaker,adding 1%ba and re filter it all..the filter i bough sucked also,it started to fall apart,and its a good name brand so i dont get that one

 

[HAYEZ]

the filter was disintegrating as you were filtering?

did you use a needle to vent it while you were baking it?

if so get another .20 whatman and refilter everything...you didnt add anything other then the ba bb and gso did you?
ive had filters disintegrate on me before..idk why it happened it was filtering eq..

in all reality the powder could of had some contamination in it to start with..refilter into a sterile vial, if its moisture then atleast its sterile moisture and prob nothing that can do any harm injected..if it was ml oil and .25ml water per shot id toss it..but prob just few drops

 

[thelocal]

yea ima have to redo it all..if it is water its not much water its still very thick ,like gsoo is

the filter was desgratign but its just wasn't that good,the receiver flask and all was falling apart and i didnt have to much pressure form my pump.it was just a bad filter..but it did have alot of air exposer while i was filling up my vials,my plan was to use a 60ml sriange and do 6 vials at a time,that didnt work the syringae just would not work had to much presure,all i had besides that was 3ml ones,so i was using a 3ml syringe to put 100ccs in each vial..had alo of air exporse could of got contaminated

 

[HAYEZ]

get a 10ml syringe and a .20 whatman from get pinz, filter each one with the syringe filter...it will go by quick...ur vials not sealed and sterile to begin or u crimping them?

 

[thelocal]

there sealed and sterile,i buy them like that..ima buy all new vials to,dont want to put them in the old ones if that are contaminated

 

[thelocal]

whats the best way to clean and make sure my beaker is sterile?

usually just add a cc of ba and get a achol swab,wipe it down,throw it in the oven for like 20 mins

 

[superflex02]

best way to sterilize your glass is an alcohol wash and baking it.

 

[HAYEZ]

beaker dont need be sterile,just heat oil slightly and suck it up in the 10 ml syringe and filter thru .20 into the vial directly. not ideal way but ur kinda fucked at this point