air in sterile vials?

[essentials]

just created a batch of 200ml of tren eth

im using sterile vials ect inserting a 22-25g while injecting the liquid into vial to relieve pressure

although the vial is not full ( approx vial holds 14ml est ),

as i shake the liquid around the vial it leaves like a residue that doesnt go no matter how long left..what is this? air?

when you look at other ug labs gear u dont see this

im just wondering what have i done wrong
im not injecting air into the vial atall just a 10ml syringe filled with solution

how do i get rid of residue?

put into oven with the rubber vented for 25-30mins at 200oC?

 

[essentials]

forgot to say

filtered using .22 millipore filter unit with septa rubber cap to allow drawing fluid into syringe then transferring into sterile vial

 

[goal245]

Not sure what residue you're talking about. Im guessing your juice crashed, what recipe did you use and what concentration did you make

 

[essentials]

not it hasnt crashed

made a batch of test eth 200 20%BB, 3%BA

il take a pic and upload

 

[essentials]

heres the image

you can clearly see this residue still there even after 2-5 hours of it just sitting in this position
with other ug vials i dont notice the slightest

http://img704.imageshack.us/img704/8347/dsc00759r.jpg

IMAGE OF VIAL ABOVE

PLEASE HELP GUYS

ALTHOUGH ITS FOR MYSELF I FEEL LET DOWN BY FINISHED PRODUCT

 

[pip88]

what oil did you use?

 

[Para_Shoot]

It even looks like theres tracks and spots of water in there.

 

[essentials]

cottonseed oil

 

[pip88]

The same thing happens to a few of my vials. I think it is either un soluble ba or bb that has evaporated.