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easy recipe
- Thread starter jochensa
- Start date
rakasha681
New member
jochensa said:
Read this forum. End.
For the most part, any recipe will be easy enough for a 4th grader to follow.
There is a great collection of posts that Kian put up, i just bumped it to the top for you.
Example recipe for EQ, simplified and dumbed down:
Take 5g EQ powder(its actually a liquid) and put it in a vial, add .75ml of BA(3%), add 20.50ml of sterile oil, shake it around a bit, use a .45u whatman syringe filter to filter it all into a new sealed sterile vial. Done. Now you have a vial with 25ml of EQ at 200mg/ml... cant get any easier than that.
lanky
Well-known member
here is my synth that i made/posted 2 years ago-
A suspension of 10 g. of 17a methyl dht 'in 500 cc. of anhydrous benzene mix with 10 cc. of ethyl formate and 3 g. of sodium hydride and stir mixture for 5 hours under an atm of nitrogen and at approximately 25 degree C. then filter suspension, the resulting mixture of the sodiumsalt of the hydroxymethylene compound and the excess of sodium hydride can be washed with benzene and dried( under a hood please, or larger ventilation system in large scale production). slowly add mixture to a vigorously stirred solution of 20 cc. of concentrated hydrochloric acid in 500 cc. of water, continue stiring for 30 minutes(eat a chicken breast while waiting, cook it on a bunson burner while you wait, dont let your boss find out,,season the chicken breast with some NaCl,,,mmmmm yumm..ionic chicken), collect precipitate and wash with distilled water. After drying in vacuum you should obtain approx 9g of 2-hydroxymethylene17a methyl dihydrotestosterone.(anadrol)
weigh out 7 g. of 2-hydroxymethylene- 17a-methyl dihydrotestosterone and dissolve in 300 cc. of methanol and mix with 2.5% of a 10% palladium on charcoal catalyst. hydrogenate at approximately 25 degree C. at atmospheric pressure until the absorption of hydrogen ceased(you should have complete hydrogenation if mol ratio calculated correctly in pre experiment calculations). The catalyst can be removed by filtration, add 1g. of potassium hydroxide in 5 cc. of water to the solution which then kept for 1 hour at room temperature. 2 cc. of acetic acid can now be added, the solvent can be removed with vacuum or reduced pressure, add distilled water to the residue and the extracte with methylene dichloride. washe extract with water, dry it over anhydrous sodium sulfate and evaporate to dryness under vacuum. crystalize n stuff and you have your product 2,17 di-methyl dht.
If i was a supplement company and had the intermediate as say a 17 alpha methyl 2-ene androstane(pheraplex). i could reduce the 2-ene and form a keto enol type rxn(i hope the 3 keto is favored) and use the 17a methyl dht from there to create superdrol....im not sure what their intermediate they use is but that would be the smart thing to do,,,1 intermediate---2 products, pheraplex/superdrol ....cost effective....yes...legal for now......of course i base this knowledge on entirely nothing....im just a little paranoid and delusional
A suspension of 10 g. of 17a methyl dht 'in 500 cc. of anhydrous benzene mix with 10 cc. of ethyl formate and 3 g. of sodium hydride and stir mixture for 5 hours under an atm of nitrogen and at approximately 25 degree C. then filter suspension, the resulting mixture of the sodiumsalt of the hydroxymethylene compound and the excess of sodium hydride can be washed with benzene and dried( under a hood please, or larger ventilation system in large scale production). slowly add mixture to a vigorously stirred solution of 20 cc. of concentrated hydrochloric acid in 500 cc. of water, continue stiring for 30 minutes(eat a chicken breast while waiting, cook it on a bunson burner while you wait, dont let your boss find out,,season the chicken breast with some NaCl,,,mmmmm yumm..ionic chicken), collect precipitate and wash with distilled water. After drying in vacuum you should obtain approx 9g of 2-hydroxymethylene17a methyl dihydrotestosterone.(anadrol)
weigh out 7 g. of 2-hydroxymethylene- 17a-methyl dihydrotestosterone and dissolve in 300 cc. of methanol and mix with 2.5% of a 10% palladium on charcoal catalyst. hydrogenate at approximately 25 degree C. at atmospheric pressure until the absorption of hydrogen ceased(you should have complete hydrogenation if mol ratio calculated correctly in pre experiment calculations). The catalyst can be removed by filtration, add 1g. of potassium hydroxide in 5 cc. of water to the solution which then kept for 1 hour at room temperature. 2 cc. of acetic acid can now be added, the solvent can be removed with vacuum or reduced pressure, add distilled water to the residue and the extracte with methylene dichloride. washe extract with water, dry it over anhydrous sodium sulfate and evaporate to dryness under vacuum. crystalize n stuff and you have your product 2,17 di-methyl dht.
If i was a supplement company and had the intermediate as say a 17 alpha methyl 2-ene androstane(pheraplex). i could reduce the 2-ene and form a keto enol type rxn(i hope the 3 keto is favored) and use the 17a methyl dht from there to create superdrol....im not sure what their intermediate they use is but that would be the smart thing to do,,,1 intermediate---2 products, pheraplex/superdrol ....cost effective....yes...legal for now......of course i base this knowledge on entirely nothing....im just a little paranoid and delusional
rakasha681
New member
lanky said:
ha! Thats great
why do you dry it over sodium sulfate instead of magnesium sulfate?
lanky
Well-known member
rakasha681 said:ha! Thats great
why do you dry it over sodium sulfate instead of magnesium sulfate?
I have no idea anymore...O chem is one of those things (use it or loose it)...and i have lost it. .could dry the stuff better, less expensive, less needed, "safer" , or course when dealing with anything it is all about the $$$$$$$$$$(because unfortunatly that is what it is all about).
