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rrash283
New member
I found this on another board and the it looks like an interesting way to remove the estrogen from syno. Only problem is its written a bit to technical for me.
"Oddly enough, it is simply using a 4 molar equivalent of NaOH to the amount of estradiol benzoate present in the solution. I would dissolve about 20g of syno in about 400mL of methanol, filter the binders (through celite using suction), and slowly drop in the 4 molar Equipoise - boldenone undecylenate - . of NaOH in a 0.5M solution from a buret while stirring the solution. I would let the solution stand (stirring was optional) for about an hour, then pour the solution into about 1L of 1M NaOH solution. After vigorously shaking the solution in a circular motion (to cause the nasty colloid to form very large clumps), I would simply filter it using a coffee filter and rinse a couple times with 1M NaOH, then finally many times with water until the powder and filter were odorless, and the filtrate was colorless. I usually sat the soaking wet filter on a towel to pull as much water out, then stapled it and rubberbanded it to a floor fan to dry for a day or two. I usually recrystallized the stuff from methanol and water after this, but it wasn't necessary as the powder was fairly pure. The whole procedure worked quite well; my genetically gifted, purely mesomorphic friend blew up on the stuff.
It was a lot of fun, but I would probably just flash chromotography the stuff if I ever wanted to get test testosterone propionate from syno."
I had a few specific questions;
For example what would the 4 molar equivalent of estradiol benzoate be. I understand it would depend on the amount of estradiol benzoate, but it should be a linear function. So any example would work.
Also, when he says "4 molar Equipoise - boldenone undecylenate - . of NaOH in a 0.5M solution" I'm not clear on what he means.
Any help clarifying this post to help those of us who don't have a degree in chemistry would be greatly appreciated.
Thanks
"Oddly enough, it is simply using a 4 molar equivalent of NaOH to the amount of estradiol benzoate present in the solution. I would dissolve about 20g of syno in about 400mL of methanol, filter the binders (through celite using suction), and slowly drop in the 4 molar Equipoise - boldenone undecylenate - . of NaOH in a 0.5M solution from a buret while stirring the solution. I would let the solution stand (stirring was optional) for about an hour, then pour the solution into about 1L of 1M NaOH solution. After vigorously shaking the solution in a circular motion (to cause the nasty colloid to form very large clumps), I would simply filter it using a coffee filter and rinse a couple times with 1M NaOH, then finally many times with water until the powder and filter were odorless, and the filtrate was colorless. I usually sat the soaking wet filter on a towel to pull as much water out, then stapled it and rubberbanded it to a floor fan to dry for a day or two. I usually recrystallized the stuff from methanol and water after this, but it wasn't necessary as the powder was fairly pure. The whole procedure worked quite well; my genetically gifted, purely mesomorphic friend blew up on the stuff.
It was a lot of fun, but I would probably just flash chromotography the stuff if I ever wanted to get test testosterone propionate from syno."
I had a few specific questions;
For example what would the 4 molar equivalent of estradiol benzoate be. I understand it would depend on the amount of estradiol benzoate, but it should be a linear function. So any example would work.
Also, when he says "4 molar Equipoise - boldenone undecylenate - . of NaOH in a 0.5M solution" I'm not clear on what he means.
Any help clarifying this post to help those of us who don't have a degree in chemistry would be greatly appreciated.
Thanks
