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TNE in Oil Experiment

DRG_

New member
I tried to brew TNE in Oil at 100mg/ml.

I have been brewing TNE in water but am unhappy with the solid matter I through away towards the bottom of each vial. I am looking for a better way to suspend with less waste. I cannot filter my TNE in water cause it solidifies in the filter.

I didn't have a recipe for TNE in oil so I copied my TNE in Water Recipe:

TNE Powder 4g
BB: 10% 4ml
BA:2% .8ml
Polysorbate80: 3% 1.2ml
Oil 31ml


It semi-solidified within five minute of filtering. I could not shake it to liquid again.

The next day I added BB to total 20% BB and PSB80 to total 6% PSB80, heated the vial and it remained suspended.

I have injected it three times now. I have felt injection pain before. I have used a lot of suspension and have injected PGF2a, which is VERY painful.

But this stuff wiped me out. It was very painful and caused major swelling. I have been eating ibuprofen to deal with the pain and wearing loose clothing to hide the absurdly swollen body parts. :)

Any ideas?
 
DRG_ said:
I tried to brew TNE in Oil at 100mg/ml.

I didn't have a recipe for TNE in oil so I copied my TNE in Water Recipe:

TNE Powder 4g
BB: 10% 4ml
BA:2% .8ml
Polysorbate80: 3% 1.2ml
Oil 31ml

Any ideas?

did you say this is the same as your TNE water recipe, except w/ Oil? so all other numbers are correct, except you use 31ml's water instead of oil?

I've been trying to find a TNE recipe. where do you get polysorbate80?
 
Illuminati said:
did you say this is the same as your TNE water recipe, except w/ Oil? so all other numbers are correct, except you use 31ml's water instead of oil?

I've been trying to find a TNE recipe. where do you get polysorbate80?


Yes, same as in oil.

Concentration 100.0 mg/ml
Total Volume 40.0 ml
Powder 4.0 Grams
BA 0.8 ml@2%
BB 4.0 ml
PSB80 1.2 ml
Oil/Water 31.0 ml

You put the (filtered)water and ba in the vials, heat the powder, bb and PSB.

Add the heated mixture to the vials 1ml at a time and shake well.

I get PSB80 from Research Supply.
 
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